alpha-Hydroxyacetophenone → HCID 17764628, compound
Reaction equation
O[CH2:2][C:3]([C:5]1[CH:10]=[CH:9][CH:8]=[CH:7][CH:6]=1)=O.[CH3:11][C:12]1([CH3:20])[CH2:17][CH2:16][C:15](=[O:18])[CH2:14][C:13]1=[O:19]>>[CH3:11][C:12]1([CH3:20])[C:13]2[O:19][CH:2]=[C:3]([C:5]3[CH:10]=[CH:9][CH:8]=[CH:7][CH:6]=3)[C:14]=2[C:15](=[O:18])[CH2:16][CH2:17]1Participants
3
Procedure
The subtitle compound was prepared according to the procedure of example 2 using hydroxyacetophenone instead of acetol and 4,4-dimethyl-1,3-cyclohexanedione instead of 1,3-cyclohexanedione in step 1.
Sources & evidence
- ORD record
- ord-6978e482304f4ba7af93015a5be48ad2
- Source dataset
- uspto-grants-2004_02
- Patent number
- US06696470B2
Reaction notes
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