HCID 23434225, compound → HCID 23434209, compound

HRID 2121749Notes

Reaction equation

HRID 2121749 reaction equation
[N+:1]([C:4]1[CH:5]=[C:6]([C:16]2[CH:21]=[CH:20][CH:19]=[CH:18][CH:17]=2)[CH:7]=[CH:8][C:9]=1[N:10]1[CH:14]=[N:13][C:12](=[O:15])[NH:11]1)([O-])=O>C(O)C.[Pd]>[NH2:1][C:4]1[CH:5]=[C:6]([C:16]2[CH:21]=[CH:20][CH:19]=[CH:18][CH:17]=2)[CH:7]=[CH:8][C:9]=1[N:10]1[CH:14]=[N:13][C:12](=[O:15])[NH:11]1

Participants

4

Reactant 1

HCID 23434225HCID 23434225, compound

Product 1

HCID 23434209HCID 23434209, compound

Reagents, catalysts & solvents 2

HCID 23938PalladiumCatalystHCID 702EthanolSolvent

Procedure

A solution of 1-(3-nitro-4-biphenylyl)-1,2-dihydro-1,2,4-triazol-3-one in 96% ethanol (25 mL) was hydrogenated over 5% palladium on charcoal to give the desired amine.

Sources & evidence

ORD record
ord-ec3b5244e90f477087f6609279daa8ab
Source dataset
uspto-grants-2004_02
Patent number
US06696475B2

Reaction notes

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