HuagongsheHuagongshe Chemistry Print Report · For research reference only
3-Bromophenyl isocyanate → HCID 22243803, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 3-Bromophenyl isocyanate | HCID 141001 | — |
| Reactant | HCID 22386590 | HCID 22386590 | — |
| Solvent | Dichloromethane | HCID 6344 | — |
| Product | HCID 22243803 | HCID 22243803 | 83.3% |
Reaction Steps
4-Amino-5-(4-methoxyphenoxy)quinazoline (0.35 g, 1.3 mmol) and 3-bromophenyl isocyanate (0.31 g, 1.6 mmol) were reacted in 20 ml of dichloromethane according to procedure E to give 1-[5-(4-methoxyphenoxy)quinazolin-4-yl]-3-(3-bromophenyl)urea (0.5 g, 83.3%, m.p. 249-251° C.).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06696482B2 |
| Source dataset | uspto-grants-2004_02 |
| ORD ID | ord-7b6865f222b340f3bc1ed8231a64ef0c |
| Source note | uspto-grants-2004_02 |