HCID 131724353, compound → HCID 10246184, compound

Participants

Reaction Steps

A mixture of the product from step E (0.20 g, 0.56 mmol) and palladium-on-carbon (10%, 0.02 g) in methanol (20 mL) was placed under an atmosphere of hydrogen and stirred overnight. The mixture was filtered, evaporated, and treated with 2 N HCl in ethanol. Evaporation of this solution to dryness to give an amorphous solid (0.18 g, 80%): LCMS (+ESI) m/z 333 (M+H).

Provenance & Evidence