HuagongsheHuagongshe Chemistry Print Report · For research reference only
Trichloroacetyl chloride → 2-(Trichloroacetyl)pyrrole
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Trichloroacetyl chloride | HCID 6420 | — |
| Reactant | Pyrrole | HCID 8027 | — |
| Solvent | Diethyl Ether | HCID 3283 | — |
| Product | 2-(Trichloroacetyl)pyrrole | HCID 321487 | 85% |
Reaction Steps
The strategy for the synthesis of polymer 8 is outlined in SCHEME 1. Pyrrole was treated with trichloroacetyl chloride in ether to give compound 1 in 85% yield. The methyl ester of this compound (2) was formed by reacting compound 1 with sodium methoxide in refluxing methanol, achieving yields of 71%.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06696575B2 |
| Source dataset | uspto-grants-2004_02 |
| ORD ID | ord-0a403ec93f7f44e9a43fc3870ceaff62 |
| Source note | uspto-grants-2004_02 |