HuagongsheHuagongshe Chemistry Print Report · For research reference only
Phenethylamine, 4-(benzyloxy)-3-methoxy- → 3-Methoxytyramine
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Phenethylamine, 4-(benzyloxy)-3-methoxy- | HCID 200382 | — |
| Reactant | HCID 178418361 | HCID 178418361 | — |
| Catalyst | Palladium | HCID 23938 | — |
| Solvent | Tetrahydrofuran | HCID 8028 | — |
| Product | 3-Methoxytyramine | HCID 1669 | — |
Reaction Steps
0.5 g of palladium on charcoal (10%) were added to 5 g (19.5 mmol) of 2-[4-(benzyloxy)-3-methoxyphenyl]ethylamine [cf.: Heterocycles, Vol. 28, 297-298 (1989)] in 100 ml of tetrahydrofuran and the mixture was hydrogenated under atmospheric pressure. After the uptake of hydrogen had ended, the mixture was filtered and the filtrate was freed from the solvent.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06696607B2 |
| Source dataset | uspto-grants-2004_02 |
| ORD ID | ord-ee8b5c659abf4372883248b7b14ea969 |
| Source note | uspto-grants-2004_02 |