Sodium ion → 4-(2-Bromo-5-methoxybenzylidene)-1-Boc-piperidine

HRID 2129616Notes

Reaction equation

HRID 2129616 reaction equation
[Br:3][c:4]1[c:5]([CH2:6][P:7](=[O:8])([O:9][CH2:10][CH3:11])[O:12][CH2:13][CH3:14])[cH:15][c:16]([O:19][CH3:20])[cH:17][cH:18]1.[C:21]([CH3:22])([CH3:23])([CH3:24])[O:25][C:26](=[O:27])[N:28]1[CH2:29][CH2:30][C:31](=[O:34])[CH2:32][CH2:33]1.[CH3:35][O:36][CH2:37][CH2:38][O:39][CH3:40].[H-:1].[Na+:2].[OH2:41]>>[Br:3][c:4]1[c:5]([CH:6]=[C:31]2[CH2:30][CH2:29][N:28]([C:26]([O:25][C:21]([CH3:22])([CH3:23])[CH3:24])=[O:27])[CH2:33][CH2:32]2)[cH:15][c:16]([O:19][CH3:20])[cH:17][cH:18]1

Participants

7

Reactant 6

HCID 923Sodium ionHCID 962WaterHCID 80711,2-DimethoxyethaneHCID 166653HydrideHCID 735900tert-Butyl 4-oxopiperidine-1-carboxylateHCID 22675346Diethyl 2-bromo-5-methoxybenzylphosphonate

Product 1

HCID 226754064-(2-Bromo-5-methoxybenzylidene)-1-Boc-piperidine

Sources & evidence

ORD record
ord-da230f3bb01f4ce99e962712eeda0ad9
Source dataset
Training data from https://doi.org/10.1039/C8SC04228D (4/10)

Reaction notes

Loading…