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HRID21424

反应详情

EQUATION

反应方程式

HRID 21424 的结构方程式

REACTANTS

反应物

2
结构：O=S(Cl)Cl
HCID24386

Thionyl chloride

Cl2OS

结构：CCCCCCOc1ccc(-c2ccccc2)c(C(=O)O)c1
HCID23289007

未命名化合物

PRODUCTS

生成物

1
结构：CCCCCCOc1ccc(-c2ccccc2)c(C(=O)Cl)c1
HCID54340583

未命名化合物

PROCEDURE

实验过程

4-n-Hexyloxybiphenyl carboxylic acid (3.0 g) and an excessive amount of thionyl chloride were heated under refluxing for 6 hours. Unaltered thionyl chloride was distilled off to obtain 4-n-hexyloxybiphenyl carboxylic acid chloride.

WORKUP

后处理

  1. temperatureunder refluxing for 6 hours
  2. distillationUnaltered thionyl chloride was distilled off