Thionyl Chloride → HCID 54340583, compound

HRID 21424Notes

Reaction equation

HRID 21424 reaction equation
[CH2:1]([O:7][C:8]1[CH:9]=[C:10]([C:20]([OH:22])=O)[C:11]([C:14]2[CH:19]=[CH:18][CH:17]=[CH:16][CH:15]=2)=[CH:12][CH:13]=1)[CH2:2][CH2:3][CH2:4][CH2:5][CH3:6].S(Cl)([Cl:25])=O>>[CH2:1]([O:7][C:8]1[CH:9]=[C:10]([C:20]([Cl:25])=[O:22])[C:11]([C:14]2[CH:19]=[CH:18][CH:17]=[CH:16][CH:15]=2)=[CH:12][CH:13]=1)[CH2:2][CH2:3][CH2:4][CH2:5][CH3:6]

Participants

3

Reactant 2

HCID 24386Thionyl ChlorideHCID 232890074-n-Hexyloxybiphenyl carboxylic acid

Product 1

HCID 54340583HCID 54340583, compound

Procedure

4-n-Hexyloxybiphenyl carboxylic acid (3.0 g) and an excessive amount of thionyl chloride were heated under refluxing for 6 hours. Unaltered thionyl chloride was distilled off to obtain 4-n-hexyloxybiphenyl carboxylic acid chloride.

Workup

  1. temperatureunder refluxing for 6 hours
  2. distillationUnaltered thionyl chloride was distilled off

Sources & evidence

ORD record
ord-7783c1004e9342cf9d5f678f9975d065
Source dataset
uspto-grants-1995_06
Patent number
US05424005

Reaction notes

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