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HRID21425

反应详情

EQUATION

反应方程式

HRID 21425 的结构方程式

REACTANTS

反应物

2
结构：CCCCCCCCOc1ccc(C(=O)O)cc1
HCID17231

4-Octyloxybenzoic acid

C15H22O3

结构：O=S(Cl)Cl
HCID24386

Thionyl chloride

Cl2OS

PRODUCTS

生成物

1
结构：CCCCCCCCOc1ccc(C(=O)Cl)cc1
HCID2760250

4-Octyloxybenzoyl chloride

C15H21ClO2

PROCEDURE

实验过程

After 4-n-octyloxybenzoic acid (11 g) and an excessive amount of thionyl chloride were heated under refluxing for 6 hours, unaltered thionyl chloride was distilled off to obtain 4-n-octyloxybenzoic acid chloride.

WORKUP

后处理

  1. temperatureunder refluxing for 6 hours
  2. distillationunaltered thionyl chloride was distilled off