HuagongsheHuagongshe Chemistry Print Report · For research reference only
Dichloromethane → 4-Octyl-biphenyl-4'-terephthalic acid chloride
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Dichloromethane | HCID 6344 | — |
| Reactant | Terephthaloyl chloride | HCID 7488 | — |
| Reactant | 2-Dimethylaminopyridine | HCID 21885 | — |
| Reactant | 4'-Octyl-[1,1'-biphenyl]-4-ol | HCID 14047211 | — |
| Solvent | Triethylamine | HCID 8471 | — |
| Product | 4-Octyl-biphenyl-4'-terephthalic acid chloride | HCID 131719017 | — |
Reaction Steps
To a solution of 4-hydroxy-4'-octylbiphenyl (0.5 g) and terephthaloyl chloride (0.36 g) in about dichloromethane (30 ml) was added drop by drop triethylamine (0.2 g). To the solution was added dimethylaminopyridine (0.013 g) and the mixture was stirred at the room temperature for 10 hours to obtain the titled compound.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05424005 |
| Source dataset | uspto-grants-1995_06 |
| ORD ID | ord-2394b2dec9d049a3b2e5b53f9d321778 |
| Source note | uspto-grants-1995_06 |