Sulfuric Acid → Ethyl 2-(2,3-dioxo-4,5-dihydro-1-benzazepin-1-yl)acetate

HRID 2147208Notes

Reaction equation

HRID 2147208 reaction equation
[CH2:1]1[NH:2][CH2:4][CH2:5][O:3][CH2:6]1.[CH:32]([Cl:33])([Cl:34])[Cl:35].[Cl:7][C:8]1([Cl:26])[C:9](=[O:25])[N:10]([CH2:19][C:20](=[O:21])[O:22][CH2:23][CH3:24])[c:11]2[c:12]([cH:15][cH:16][cH:17][cH:18]2)[CH2:13][CH2:14]1.[S:27](=[O:28])(=[O:29])([OH:30])[OH:31]>>[O:3]=[C:8]1[C:9](=[O:25])[N:10]([CH2:19][C:20](=[O:21])[O:22][CH2:23][CH3:24])[c:11]2[c:12]([cH:15][cH:16][cH:17][cH:18]2)[CH2:13][CH2:14]1

Participants

5

Reactant 4

HCID 1118Sulfuric AcidHCID 6212ChloroformHCID 8083MorpholineHCID 154880513,3-dichloro-1-ethoxycarbonylmethyl-2,3,4,5-tetrahydro-1H-[1]benzazepin-2-one

Product 1

HCID 13500724Ethyl 2-(2,3-dioxo-4,5-dihydro-1-benzazepin-1-yl)acetate

Sources & evidence

ORD record
ord-536b3ba6242d44618b36b9ce33455818
Source dataset
Training data from https://doi.org/10.1039/C8SC04228D (4/10)

Reaction notes

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