HuagongsheHuagongshe Chemistry Print Report · For research reference only
Dichloromethane → HCID 66891072, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Dichloromethane | HCID 6344 | — |
| Reactant | HCID 86598724 | HCID 86598724 | — |
| Solvent | Trifluoroacetic acid | HCID 6422 | — |
| Product | HCID 66891072 | HCID 66891072 | — |
Reaction Steps
A solution of the product of Example 286B (0.35 g) in trifluoroacetic acid:dichloromethane (3 mL, 2:1) was stirred at 25° C. for 2 hrs. The solvents were evaporated and the residue was directly used for the next step.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08193227B2 |
| Source dataset | uspto-grants-2012_06 |
| ORD ID | ord-d8678e7cbc774c08968401b125268730 |
| Source note | uspto-grants-2012_06 |