HuagongsheHuagongshe Chemistry Print Report · For research reference only
N-bromobutanimide → 1-Bromo-2-(bromomethyl)-3-(trifluoromethyl)benzene
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | N-bromobutanimide | HCID 67184 | — |
| Reactant | alpha,alpha,alpha-Trifluoro-3-nitro-o-xylene | HCID 81171 | — |
| Reactant | 1-Bromo-2-methyl-3-(trifluoromethyl)benzene | HCID 2775634 | — |
| Product | 1-Bromo-2-(bromomethyl)-3-(trifluoromethyl)benzene | HCID 22754136 | — |
Reaction Steps
The methyl group of 2-bromo-6-trifluoromethyltoluene was brominated by reacting 47.8 g. of the toluene with 39.2 g. of N-bromosuccinimide under ultraviolet radiation. 77.5 g. of an orange oil comprising 2-bromo-6-trifluoromethylbenzyl bromide were obtained.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04132737 |
| Source dataset | uspto-grants-1979_01 |
| ORD ID | ord-99383017395a4336a01927d0ad5d6d9c |
| Source note | uspto-grants-1979_01 |