HuagongsheHuagongshe Chemistry Print Report · For research reference only
Acetonitrile → 4-(2,2-dimethylpropyl)-2-methyl-1H-imidazol-1-ol
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Acetonitrile | HCID 6342 | — |
| Reactant | 4,4-Dimethylpent-1-ene | HCID 12984 | — |
| Reactant | Nitrilooxonium tetrafluoroborate | HCID 11137142 | — |
| Product | 4-(2,2-dimethylpropyl)-2-methyl-1H-imidazol-1-ol | HCID 68667641 | — |
Reaction Steps
4,4-Dimethyl-1-pentene (59 g, 0.6 mol) was added to a 10° C. suspension of nitrosonium tetrafluoroborate (66 g, 0.56 mmol) in acetonitrile (600 mL) After stirring vigorously at ambient temperature for 30 minutes, acetonitrile was removed in vacuo to afford 4-(2,2-dimethylpropyl)-2-methyl-1H-imidazol-1-ol which was used in the subsequent step without further purification.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08193228B2 |
| Source dataset | uspto-grants-2012_06 |
| ORD ID | ord-8f275411a5eb43a3b0991880d70309c4 |
| Source note | uspto-grants-2012_06 |