1-Bromohexadecane → HCID 178516453, compound

Participants

Reaction Steps

Using 11.6 g of 2,4-dichloro-5-(4-nitrophenoxy)-aniline hydrochloride and 13.1 g of 1-(2,4,6-trichlorophenyl)-3-ethoxy-2-pyrazolin-5-one, which were prepared in a manner similar to Steps (1) and (2) of Synthesis Example 1 except that 21.2 g of 4-fluoronitrobenzene was used in lieu of hexadecyl bromide in Step (1) of Synthesis Example 1, procedures similar to Step (3) of Synthesis Example 1 were carried out. In this case, 10.0 g of the desired product was obtained without recrystallization. The melting point thereof was 305 to 306° C.

Provenance & Evidence