HuagongsheHuagongshe Chemistry Print Report · For research reference only
Potassium Iodide → 3-Bromopropyl-2-n-butylphenyl ether
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Potassium Iodide | HCID 4875 | — |
| Reactant | 1,3-Dibromopropane | HCID 8001 | — |
| Reactant | Potassium Carbonate | HCID 11430 | — |
| Reactant | 2-Butylphenol | HCID 18515 | — |
| Solvent | Acetone | HCID 180 | — |
| Product | 3-Bromopropyl-2-n-butylphenyl ether | HCID 70605999 | — |
Reaction Steps
A solution of 30 parts of o-n-butylphenol in 150 parts of dry acetone was added dropwise over 5 hours to a stirred refluxing suspension of 80.8 parts of 1,3-dibromopropane, 27.6 parts of anhydrous potassium carbonate and 0.5 parts of potassium iodide in 170 parts of dry acetone.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04133889 |
| Source dataset | uspto-grants-1979_01 |
| ORD ID | ord-84cd0fa74cdd43878d052ba48a60014f |
| Source note | uspto-grants-1979_01 |