HuagongsheHuagongshe Chemistry Print Report · For research reference only
5-Amino-3,4-dimethylisoxazole → HCID 54694110, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 5-Amino-3,4-dimethylisoxazole | HCID 88317 | — |
| Reactant | 2H-Thieno(2,3-e)-1,2-thiazine-3-carboxylic acid, 4-hydroxy-2-methyl-, methyl ester, 1,1-dioxide | HCID 54690599 | — |
| Product | HCID 54694110 | HCID 54694110 | — |
Reaction Steps
By reacting 5-amino-3,4-dimethyl-isoxazole with 3-carbomethoxy-4-hydroxy-2-methyl-thieno[2,3-e]-1,2-thiazine 1,1-dioxide for 14 hours in a manner analogous to that described in Example 1, there is obtained N-(3,4-dimethyl-5-isoxazolyl)-4-hydroxy-2-methyl-2H-thieno[2,3-e]-1,2-thiazine-3-carboxamide 1,1-dioxide of decomposition point 206°-208° C. (recrystallization from benzene.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04134898 |
| Source dataset | uspto-grants-1979_01 |
| ORD ID | ord-38a14212763a4dab9f487afa5eaf3f24 |
| Source note | uspto-grants-1979_01 |