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HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 2163526Generated: November 3, 2026

1-Bromo-3-chloropropane → HCID 22752798, compound

https://huagongshe.com/reaction/2163526

Reaction equation

Participants

RoleNameHCIDCharge
Reactant1-Bromo-3-chloropropaneHCID 8006—
ReactantChloroform methanolHCID 21584188—
ReactantHCID 22752786HCID 22752786—
SolventDimethylformamideHCID 6228—
ProductHCID 22752798HCID 22752798—

Reaction Steps

1-[4-Isopropyl-6,7-dimethoxy-1(2H)-phthalazinone-2-yl]-3-chloro-propane was prepared analogous to Example 1 (a) by reaction of 4-isopropyl-6,7-dimethoxy-1(2H)-phthalazinone with 1-bromo-3-chloro-propane in dimethylformamide. Rf -value (chloroform/methanol = 50/1) : 0.5.

Provenance & Evidence

DOI10.6084/m9.figshare.5104873.v1
Patent numberUS04134980
Source datasetuspto-grants-1979_01
ORD IDord-667bece09e294421a15dff9c4c0aae1e
Source noteuspto-grants-1979_01