4-Methoxy-N-methylbenzeneethanamine → HCID 22752796, compound

HRID 2163528Notes

Reaction equation

HRID 2163528 reaction equation
[CH3:1][C:2]1[C:11]2[C:6](=[CH:7][C:8]([O:14][CH3:15])=[C:9]([O:12][CH3:13])[CH:10]=2)[C:5](=[O:16])[N:4]([CH2:17][CH2:18][CH2:19][Cl:20])[N:3]=1.[CH3:21][O:22][C:23]1[CH:28]=[CH:27][C:26]([CH2:29][CH2:30][NH:31][CH3:32])=[CH:25][CH:24]=1>ClC1C=CC=CC=1>[ClH:20].[CH3:1][C:2]1[C:11]2[C:6](=[CH:7][C:8]([O:14][CH3:15])=[C:9]([O:12][CH3:13])[CH:10]=2)[C:5](=[O:16])[N:4]([CH2:17][CH2:18][CH2:19][N:31]([CH3:32])[CH2:30][CH2:29][C:26]2[CH:27]=[CH:28][C:23]([O:22][CH3:21])=[CH:24][CH:25]=2)[N:3]=1

Participants

4

Reactant 2

HCID 1047354-Methoxy-N-methylbenzeneethanamineHCID 22752785HCID 22752785, compound

Product 1

HCID 22752796HCID 22752796, compound

Reagents, catalysts & solvents 1

HCID 7964ChlorobenzeneSolvent

Procedure

Produced analogously to Example 2 (b) by reaction of 1-[4-methyl-6,7-dimethoxy-1-(2H)-phthalazinone-2-yl]-3-chloro-propane with N-(4-methoxy-phenylethyl)-N-methyl-amine in chlorobenzene. M. p.: 210 - 212° C.

Sources & evidence

ORD record
ord-ebeccdff8e7c42578ecf04d913d1f253
Source dataset
uspto-grants-1979_01
Patent number
US04134980

Reaction notes

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