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HRID2163529

反应详情

EQUATION

反应方程式

HRID 2163529 的结构方程式

REACTANTS

反应物

3
结构：ClCCCBr
HCID8006

1-Bromo-3-chloropropane

C3H6BrCl

结构：COc1cc2cn[nH]c(=O)c2cc1OC
HCID12298545

6,7-Dimethoxyphthalazin-1(2H)-one

C10H10N2O3

结构：CO.ClC(Cl)Cl
HCID21584188

Chloroform methanol

C2H5Cl3O

PRODUCTS

生成物

1
结构：COc1cc2cnn(CCCCl)c(=O)c2cc1OC
HCID22150171

未命名化合物

AUXILIARIES

试剂、催化剂与溶剂

1
结构：CN(C)C=O
溶剂HCID6228

N,N-Dimethylformamide

C3H7NO

PROCEDURE

实验过程

1-[6,7-Dimethoxy-1(2H)-phthalazinone-2-yl]-3-chloro-propane was prepared analogous to Example 1 (a) by reaction of 6,7-dimethoxy-1(2H)-phthalazinone with 1-bromo-3-chloro-propane in dimethylformamide. Rf -value (chloroform/methanol = 9/1) : 0.9.