Benzhydrylamine → HCID 178480596, compound

HRID 2163672Notes

Reaction equation

HRID 2163672 reaction equation
[CH:1]([NH2:14])([C:8]1[CH:13]=[CH:12][CH:11]=[CH:10][CH:9]=1)[C:2]1[CH:7]=[CH:6][CH:5]=[CH:4][CH:3]=1.[IH:15].[CH3:16][N:17]1[CH2:21][CH2:20][N:19]=[C:18]1SC>>[IH:15].[CH3:16][N:17]1[CH2:21][CH2:20][NH:19][C:18]1=[N:14][CH:1]([C:8]1[CH:9]=[CH:10][CH:11]=[CH:12][CH:13]=1)[C:2]1[CH:7]=[CH:6][CH:5]=[CH:4][CH:3]=1

Participants

3

Reactant 2

HCID 7036BenzhydrylamineHCID 122815051-methyl-2-(methylsulfanyl)-4,5-dihydro-1H-imidazole hydroiodide

Product 1

HCID 178480596HCID 178480596, compoundYield 31.1%

Procedure

A mixture of 1.8 g of benzhydrylamine and 3.4 g of 1-methyl-2-methylmercapto-2-imidazoline.hydroiodide was allowed to stand at room temperature for 2 days. Chloroform was then distilled off to give 1.2 g of 1-methyl-2-benzhydryliminoimidazolidine.hydroiodide having a melting point of 254°-256° C.

Workup

  1. distillationChloroform was then distilled off

Sources & evidence

ORD record
ord-0d4a7604f3ee4795a69d3d3fc50a69c9
Source dataset
uspto-grants-1979_01
Patent number
US04136188

Reaction notes

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