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HRID2163769

反应详情

EQUATION

反应方程式

HRID 2163769 的结构方程式

REACTANTS

反应物

3
结构：CC(C)=O
HCID180

Acetone

C3H6O

结构：CCCCCCCCCCCCCCCCNc1ccc(C(=O)Cl)cc1.Cl
HCID13255322

未命名化合物

结构：NC(N)=O.[Na]
HCID86736265

未命名化合物

PRODUCTS

生成物

1
结构：CCCCCCCCCCCCCCCCNc1ccc(C(=O)NC(N)=O)cc1
HCID20437348

未命名化合物

AUXILIARIES

试剂、催化剂与溶剂

1
结构：ClCCl
溶剂HCID6344

Dichloromethane

CH2Cl2

PROCEDURE

实验过程

The 12.6 g. of 4-(hexadecylamino)benzoyl chloride hydrochloride in methylene chloride is added to 5 g. of sodium urea in 30 ml. of acetone and the mixture is stirred at 20° C. for 18 hours. Dilute alkali is added and the solid washed with alkaline aqueous acetone. Recrystallization from ethanol gives pure white crystals of product.

WORKUP

后处理

  1. additionDilute
  2. additionalkali is added
  3. washthe solid washed with alkaline aqueous acetone
  4. customRecrystallization from ethanol
  5. customgives pure white crystals of product