HuagongsheHuagongshe Chemistry Print Report · For research reference only
Ethylenediamine → N-(3-isothiazolylmethyl)ethylenediamine
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Ethylenediamine | HCID 3301 | — |
| Reactant | 3-(bromomethyl)Isothiazole | HCID 13037598 | — |
| Product | N-(3-isothiazolylmethyl)ethylenediamine | HCID 20557777 | — |
Reaction Steps
By the procedure of Example 34, ethylenediamine is reacted with 3-bromomethylisothiazole to give N-(3-isothiazolylmethyl)ethylenediamine. This intermediate is heated under reflux with S-methylisothiouronium sulphate in water for 3 hours by the procedure of Example 1 to give the title compound.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04137237 |
| Source dataset | uspto-grants-1979_01 |
| ORD ID | ord-54b00dfe6201431999a92077646a3358 |
| Source note | uspto-grants-1979_01 |