Aniline → HCID 54684925, compound

HRID 2164109Notes

Reaction equation

HRID 2164109 reaction equation
[CH3:1][N:2]1[C:15]([C:16](OC)=[O:17])=[C:14]([OH:20])[C:5]2[N:6]([CH3:13])[C:7]3[CH:8]=[CH:9][CH:10]=[CH:11][C:12]=3[C:4]=2[S:3]1(=[O:22])=[O:21].[NH2:23][C:24]1[CH:29]=[CH:28][CH:27]=[CH:26][CH:25]=1>C1(C)C=CC=CC=1>[CH3:1][N:2]1[C:15]([C:16]([NH:23][C:24]2[CH:29]=[CH:28][CH:27]=[CH:26][CH:25]=2)=[O:17])=[C:14]([OH:20])[C:5]2[N:6]([CH3:13])[C:7]3[CH:8]=[CH:9][CH:10]=[CH:11][C:12]=3[C:4]=2[S:3]1(=[O:21])=[O:22]

Participants

4

Reactant 2

HCID 6115AnilineHCID 54684931HCID 54684931, compound

Product 1

HCID 54684925HCID 54684925, compound

Reagents, catalysts & solvents 1

HCID 1140TolueneSolvent

Procedure

2,5-Dihydro-2,5-dimethyl-4-hydroxy-N-phenyl-1,2-thiazino [5,6-b]-indole-3-carboxamide-1,1-dioxide was prepared analogous to Example 9 from methyl 2,5-dihydro-2,5-dimethyl-4-hydroxy-1,2-thiazino[5,6-b]indole-3-carboxylate-1,1-dioxide and aniline in toluene; M.p.: 269°-270° C. (decomposition);

Sources & evidence

ORD record
ord-91c541009e6e468ca0d89996c8e41597
Source dataset
uspto-grants-1979_01
Patent number
US04137313

Reaction notes

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