HuagongsheHuagongshe Chemistry Print Report · For research reference only
Thionyl Chloride → HCID 22750308, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Thionyl Chloride | HCID 24386 | — |
| Reactant | HCID 22750325 | HCID 22750325 | — |
| Solvent | Dimethylformamide | HCID 6228 | — |
| Product | HCID 22750308 | HCID 22750308 | — |
Reaction Steps
From 7.0 g. of 6-[4-(2-pyridylaminosulfonyl)phenyl]-1,2-dihydro-2-oxonicotinic acid in 200 ml. of thionyl chloride, and 1.5 ml. of dimethylformamide, following the procedure of c) above, there is obtained 6-[4-(2-pyridylaminosulfonyl)phenyl]-1,2-dihydro-2-oxonicotinyl chloride hydrochloride.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04137408 |
| Source dataset | uspto-grants-1979_01 |
| ORD ID | ord-88b8b7935a8b4136a1c410e46e037066 |
| Source note | uspto-grants-1979_01 |