HCID 22749736, compound → HCID 53773602, compound

HRID 2164184Notes

Reaction equation

HRID 2164184 reaction equation
C([Cl:9])(=O)C1C=CC=CC=1.C1(OP(OC2C=CC=CC=2)OC2C=CC=CC=2)C=CC=CC=1.[CH3:32][C:33]([CH2:40][CH3:41])=[CH:34][CH2:35][CH2:36][CH:37](O)[CH3:38]>>[Cl:9][CH:37]([CH2:36][CH2:35][CH:34]=[C:33]([CH3:32])[CH2:40][CH3:41])[CH3:38]

Participants

3

Reactant 2

HCID 22749736HCID 22749736, compoundHCID 54451138HCID 54451138, compound

Product 1

HCID 53773602HCID 53773602, compound

Procedure

Triphenylphosphite benzoylchloride (10 g.) is mixed with 1.9 g. of 6-methyl-5-octen-2-ol and kept at room temperature overnight. The crude product is washed with 2N sodium hydroxide and water and dried to yield 2-chloro-6-methyl-5-octene.

Workup

  1. washThe crude product is washed with 2N sodium hydroxide and water
  2. customdried

Sources & evidence

ORD record
ord-ef05612bc35040d89270478d0c92df35
Source dataset
uspto-grants-1979_01
Patent number
US04137273

Reaction notes

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