Ethyl bromoacetate → HCID 21790152, compound
Reaction equation
[CH2:1]([O:3][C:4]([C:6]1[N:7]([CH3:16])[C:8]2[C:13]([C:14]=1[OH:15])=[CH:12][CH:11]=[CH:10][CH:9]=2)=[O:5])[CH3:2].Br[CH2:18][C:19]([O:21][CH2:22][CH3:23])=[O:20]>>[CH2:1]([O:3][C:4]([C:6]1[N:7]([CH3:16])[C:8]2[C:13]([C:14]=1[O:15][CH2:18][C:19]([O:21][CH2:22][CH3:23])=[O:20])=[CH:12][CH:11]=[CH:10][CH:9]=2)=[O:5])[CH3:2]Participants
3
Procedure
Prepared by the procedure described in Example 1 from 3-hydroxy-1-methyl-1H-indole-2-carboxylic acid ethyl ester and ethyl bromoacetate. The crude oil product obtained after evaporation was used for further synthesis without additional purification.
Workup
- customPrepared by the procedure
- customThe crude oil product obtained
- customafter evaporation
- customwas used for further synthesis without additional purification
Sources & evidence
- ORD record
- ord-9d1196acfee4444ca22747546903152b
- Source dataset
- uspto-grants-1985_03
- Patent number
- US04503236
Reaction notes
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