HuagongsheHuagongshe Chemistry Print Report · For research reference only
Dichlorodimethylsilane → HCID 13244761, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Dichlorodimethylsilane | HCID 6398 | — |
| Reactant | Triethylamine | HCID 8471 | — |
| Reactant | 2,2'-Ethylidenebis(4,6-di-tert-butylphenol) | HCID 118899 | — |
| Product | HCID 13244761 | HCID 13244761 | 79% |
Reaction Steps
Utilizing the procedure of Example 1, this compound is prepared from 25.8 grams (0.20 mole) of dichlorodimethylsilane, 87.7 grams (0.20 mole) of 2,2'-ethylidene-bis(4,6-di-t-butylphenol) and 40.5 grams (0.40 mole) of triethylamine. Recrystallization from acetonitrile-toluene yields 77.7 g (79% yield) of product as white needles, mp 171°-177° C.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04503243 |
| Source dataset | uspto-grants-1985_03 |
| ORD ID | ord-0e866f3d227b455e906aeccfc00df42b |
| Source note | uspto-grants-1985_03 |