Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
Triethylamine → 2,4,8,10-Tetra-t-butyl-6-phenyl-dibenzo[d,g][1,3,2,6]dioxasilathiocin
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | Triethylamine | HCID 8471 | — |
| 반응물 | Dichloro(phenyl)silane | HCID 74207 | — |
| 반응물 | 4,4',6,6'-Di-tert-butyl-2,2'-thiobisphenol | HCID 10898437 | — |
| 생성물 | 2,4,8,10-Tetra-t-butyl-6-phenyl-dibenzo[d,g][1,3,2,6]dioxasilathiocin | HCID 123476377 | 41% |
반응 단계
Utilizing the procedure of Example 1, this compound is prepared from 5.3 grams (0.03 mole) dichlorophenylsilane, 13.3 grams (0.03 mole) 2,2'-thio-bis(4,6-di-t-butylphenol), and 6.1 grams (0.06 mole) triethylamine. Recrystallization from acetone gives 6.7 grams (41% yield) of white solid, mp 175°-177° C.
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US04503243 |
| 출처 데이터셋 | uspto-grants-1985_03 |
| ORD ID | ord-9a1a3897ad3f4bc693177c5726959d68 |
| 출처 메모 | uspto-grants-1985_03 |