Participants
| Role | Name | HCID | Charge |
|---|
| Reactant | Ethylene Glycol | HCID 174 | — |
| Reactant | Formaldehyde | HCID 712 | — |
| Reactant | Water | HCID 962 | — |
| Reactant | Sulfuric Acid | HCID 1118 | — |
| Reactant | Urea | HCID 1176 | — |
| Reactant | Isobutyraldehyde | HCID 6561 | — |
| Product | HCID 23513452 | HCID 23513452 | — |
Reaction Steps
60 Parts (1.0 mole) of urea, 30 parts (1.0 mole) of paraformaldehyde, 72 parts (1.0 mole) of isobutyraldehyde, 92 parts (1.5 moles) of ethylene glycol, 46 parts (2.6 moles) of water, and 10 parts of 40% sulfuric acid were stirred together and heated at 70° C. until a clear solution of an equilibrium mixture of 5,5-dimethylpyrimid-3-en-2-one and 5,5,-dimethyl-4-hydroxyethoxypyrimid-2-one was formed, confirmed by IR spectra.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|
| Patent number | US04505712 |
|---|
| Source dataset | uspto-grants-1985_03 |
|---|
| ORD ID | ord-421caad7ab0e44478f6bb1a9e1d29aa5 |
|---|
| Source note | uspto-grants-1985_03 |
|---|
