HuagongsheHuagongshe Chemistry Print Report · For research reference only
Chlorosuccinimide → HCID 13473178, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Chlorosuccinimide | HCID 31398 | — |
| Reactant | 2-(Ethylthio)-2-methylpropanenitrile | HCID 12270745 | — |
| Solvent | Carbon Tetrachloride | HCID 5943 | — |
| Product | HCID 13473178 | HCID 13473178 | 101.5% |
Reaction Steps
In 10 ml of carbon tetrachloride were placed 1.4 g of 2-(ethylthio)-2-methylpropanenitrile and 1.5 g of N-chlorosuccinimide and the mixture was refluxed with stirring for four hours. Solid was filtered and the filtrate was evaporated to give 1.8 g of product as a yellow liquid. This product was used without purification.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04505904 |
| Source dataset | uspto-grants-1985_03 |
| ORD ID | ord-b89ed531cdc24fa4999b690a450e943d |
| Source note | uspto-grants-1985_03 |