HuagongsheHuagongshe Chemistry Print Report · For research reference only
Allylamine → HCID 86739977, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Allylamine | HCID 7853 | — |
| Reactant | Methyl 2-cyano-3,3-bis(methylsulfanyl)prop-2-enoate | HCID 319957 | — |
| Solvent | 1,2-Dimethoxyethane | HCID 8071 | — |
| Product | HCID 86739977 | HCID 86739977 | 101.5% |
Reaction Steps
To a suspension of 2-cyano-3,3-bis(methylthio)-2-propenoic acid, methyl ester (8.12 g) in dimethoxyethane (13 mL) was added (2-propenyl)amine (2.51 g). The mixture dissolved. After about 15 min the solvent was evaporated under nitrogen and the solid residue was filtered with diethyl ether to give 2-cyano-3-methylthio-3-(2-propenyl)amino-2-propenoic acid, methyl ester (8.61 g).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04505910 |
| Source dataset | uspto-grants-1985_03 |
| ORD ID | ord-573d0532c2764341b31b4329b36cb78d |
| Source note | uspto-grants-1985_03 |