HuagongsheHuagongshe Chemistry Print Report · For research reference only
Triethylamine → HCID 70486802, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Triethylamine | HCID 8471 | — |
| Reactant | Dicyclohexylcarbodiimide | HCID 10868 | — |
| Reactant | Methyl L-phenylalaninate hydrochloride | HCID 75736 | — |
| Reactant | HCID 86739993 | HCID 86739993 | — |
| Solvent | Chloroform | HCID 6212 | — |
| Solvent | Tetrahydrofuran | HCID 8028 | — |
| Product | HCID 70486802 | HCID 70486802 | — |
Reaction Steps
4-Allyloxy-3-chloro-phenylacetyl-(L)-phenylalanine (1.87 g) was dissolved in dry tetrahydrofuran (10 ml). To the solution was added (L)-phenylalanine methyl ester hydrochloride in dry chloroform (10 ml) containing dry triethylamine (0.7 ml). DCC (1.02 g) was added and the reaction mixture was stirred overnight.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04505898 |
| Source dataset | uspto-grants-1985_03 |
| ORD ID | ord-3ce289757c5f438d8a3ccefece0491b4 |
| Source note | uspto-grants-1985_03 |