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HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 2164573Generated: October 30, 2026

Triethylamine → HCID 86739455, compound

https://huagongshe.com/reaction/2164573

Reaction equation

Participants

RoleNameHCIDCharge
ReactantTriethylamineHCID 8471—
ReactantDicyclohexylcarbodiimideHCID 10868—
ReactantGlycine methyl ester hydrochlorideHCID 122755—
ReactantHCID 86739456HCID 86739456—
SolventChloroformHCID 6212—
SolventTetrahydrofuranHCID 8028—
ProductHCID 86739455HCID 86739455—

Reaction Steps

4-Allyloxy-3-chloro-phenylacetyl-(DL)-phenylalanyl-(DL)-phenylalanine (1.20 g) was dissolved in dry tetrahydrofuran (10 ml). To the solution was added glycine methyl ester hydrochloride (0.25 g) in dry chloroform (10 ml) containing dry triethylamine (0.28 ml). DCC (0.41 g) was added and the reaction mixture was stirred overnight at room temperature. DCU was then filtered off.

Provenance & Evidence

DOI10.6084/m9.figshare.5104873.v1
Patent numberUS04505898
Source datasetuspto-grants-1985_03
ORD IDord-41a9f814c9e04dd58787b493c920c5f4
Source noteuspto-grants-1985_03