Participants
| Role | Name | HCID | Charge |
|---|
| Reactant | Acetic Acid | HCID 176 | — |
| Reactant | HCID 13473207 | HCID 13473207 | — |
| Product | HCID 13473210 | HCID 13473210 | — |
Reaction Steps
A suspension of 6-(2,3-epoxypropoxy)benzothiazole-2-sulfonamide (1.57 gm, 5.5 mmol) in acetic acid (25 mL) was heated at 100° C. for 3-4 hours. The solvent was evaporated. Traces of solvent were removed by chasing with toluene. The residue was dissolved in acetonitrile and diluted with chloroform. Upon standing, product crystallized (0.77 gm), m.p. 173°-175° C.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|
| Patent number | US04505923 |
|---|
| Source dataset | uspto-grants-1985_03 |
|---|
| ORD ID | ord-a65115c870bb4286affbeafc77de5cc4 |
|---|
| Source note | uspto-grants-1985_03 |
|---|
