HuagongsheHuagongshe Chemistry Print Report · For research reference only
Dimethylformamide → HCID 11379153, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Dimethylformamide | HCID 6228 | — |
| Reactant | 2-Chloro-6-nitrotoluene | HCID 6740 | — |
| Reactant | Dimethylformamide dimethyl acetal | HCID 78373 | — |
| Solvent | Methanol | HCID 887 | — |
| Product | HCID 11379153 | HCID 11379153 | — |
Reaction Steps
A 2-liter flask fitted with a 30-cm. vacuum-jacketed Vigreux column, downward condenser, and receiver with a nitrogen inlet was charged with 171.6 g. of 6-chloro-2-nitrotoluene, 500 ml. of dimethylformamide, and 149.0 g. of N,N-dimethylformamide dimethyl acetal and then heated to 140°-156° for 13 hours. The pot temperature was maintained by continuous distillation of the methanol as it was formed.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04506078 |
| Source dataset | uspto-grants-1985_03 |
| ORD ID | ord-e06bca959a6d43c7a3c12fdf6a940393 |
| Source note | uspto-grants-1985_03 |