3,5-Dimethyl-4-nitrocyclohex-1-ene → 2,6-Dimethylcyclohexylamine

HRID 2164687Notes

Reaction equation

HRID 2164687 reaction equation
[CH3:1][CH:2]1[CH:7]([N+:8]([O-])=O)[CH:6]([CH3:11])[CH2:5][CH:4]=[CH:3]1.[H][H]>[Pd]>[CH3:11][CH:6]1[CH2:5][CH2:4][CH2:3][CH:2]([CH3:1])[CH:7]1[NH2:8]

Participants

4

Reactant 2

HCID 204053483,5-Dimethyl-4-nitrocyclohex-1-eneHCID 178418361HCID 178418361, compound

Product 1

HCID 1109322,6-Dimethylcyclohexylamine

Reagents, catalysts & solvents 1

HCID 23938PalladiumCatalyst

Procedure

contacting said 3,5-dimethyl-4-nitro-cyclohexene with hydrogen at a temperature of about 0° C. to about 200° C. and a pressure of about 0 psig to about 1500 psig in the presence of a palladium catalyst to form 2,6-dimethylcyclohexyl amine; and

Workup

  1. customat a temperature of about 0° C. to about 200° C.

Sources & evidence

ORD record
ord-cdaada7ceb2a4cfe80bb83c656bd31ab
Source dataset
uspto-grants-1985_03
Patent number
US04506098

Reaction notes

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