HuagongsheHuagongshe Chemistry Print Report · For research reference only
Hydrochloric Acid → HCID 20037736, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Hydrochloric Acid | HCID 313 | — |
| Reactant | HCID 20037725 | HCID 20037725 | — |
| Solvent | Sodium Hydroxide | HCID 14798 | — |
| Product | HCID 20037736 | HCID 20037736 | — |
Reaction Steps
A mixture of 3.8 g (0.012) of N-(3-ethylthio-2-methyl propanoyl)-N-cyclopentyl glycine ethyl ester in 80 ml of 10% NaOH was stirred for 7 hours. It was then cooled, acidified with 10% HCl, extracted with ether, dried over MgSO4, and evaporated to dryness giving oily residue which was purified by HPLC using HOAc-EtOAc-Hexane (5:45:50).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04507316 |
| Source dataset | uspto-grants-1985_03 |
| ORD ID | ord-26a14c271ee5418396a247b8ad614994 |
| Source note | uspto-grants-1985_03 |