HuagongsheHuagongshe Chemistry Print Report · For research reference only
HCID 178430866, compound → HCID 178430865, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | HCID 178430866 | HCID 178430866 | — |
| Catalyst | Palladium | HCID 23938 | — |
| Solvent | Ethanol | HCID 702 | — |
| Product | HCID 178430865 | HCID 178430865 | — |
Reaction Steps
A mixture of 23.44 g of 4-methyl-2-(2-nitrobenzyl)imidazole, 2.34 g of 10% palladium on charcoal and 234 ml of ethanol is hydrogenated at 42 psi (3 atmospheres) at room temperature for 4 hours. The catalyst is filtered and the filtrates are evaporated to dryness to give 4-methyl-2-(2-aminobenzyl)imidazole showing signals in the NMR spectrum at δ 2.09, 3.78, 6.08.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04507311 |
| Source dataset | uspto-grants-1985_03 |
| ORD ID | ord-14ad724b3b624c88b249bb38de8ad813 |
| Source note | uspto-grants-1985_03 |