HuagongsheHuagongshe Chemistry Print Report · For research reference only
1-Ethylpiperazine → HCID 54036251, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 1-Ethylpiperazine | HCID 79196 | — |
| Reactant | N-Boc-L-Leucine Hydrate | HCID 12373896 | — |
| Reactant | HCID 13455629 | HCID 13455629 | — |
| Product | HCID 54036251 | HCID 54036251 | 65% |
Reaction Steps
Tert-butoxycarbonyl-L-leucine monohydrate (7.47 g) and 1-ethylpiperazine (3.42 g) were condensed in the same manner as employed in the preparation of tert-butyl (s)-1-(4-diphenylmethylpiperazine-1-yl carbonyl)-3-methylbutylcarbamate to yield 6.4 g of tert-butyl (s)-1-(4-ethylpiperazine-1-yl carbonyl)-3-methylbutylcarbamate as a colorless viscous liquid (yield: 65%).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04507297 |
| Source dataset | uspto-grants-1985_03 |
| ORD ID | ord-21f68f3b63124d9393cb5151a9073f3e |
| Source note | uspto-grants-1985_03 |