HuagongsheHuagongshe Chemistry Print Report · For research reference only
Pyridine → HCID 23043544, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Pyridine | HCID 1049 | — |
| Reactant | 4-Toluenesulfonyl chloride | HCID 7397 | — |
| Reactant | 2-(2-(Decyloxy)ethoxy)ethanol | HCID 526731 | — |
| Solvent | Water | HCID 962 | — |
| Product | HCID 23043544 | HCID 23043544 | 80.8% |
Reaction Steps
A mixture of 116 g of 2-[2-(decyloxy)ethoxy]-ethanol, 98.73 g of tosyl chloride and 600 ml of pyridine was stored in a chill room overnight, then poured into water and extracted with ether. The ether extract was washed successively with water, dilute hydrochloric acid and dilute aqueous sodium bicarbonate, dried and the ether removed, giving 146.3 g of the desired compound as an oil.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04939127 |
| Source dataset | uspto-grants-1990_07 |
| ORD ID | ord-5a9c45da221c4e3782861cb0639d620c |
| Source note | uspto-grants-1990_07 |