HuagongsheHuagongshe Chemistry Print Report · For research reference only
Tetrahydrofuran → HCID 23043605, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Tetrahydrofuran | HCID 8028 | — |
| Reactant | HCID 54232854 | HCID 54232854 | — |
| Solvent | Methanol | HCID 887 | — |
| Product | HCID 23043605 | HCID 23043605 | 65.5% |
Reaction Steps
The 1,2-dibenzyloxy-4-[2-(4-nitrophenyl)ethenyl]benzene (10 g, 22 mmole) is dissolved in methanol (50 ml), THF (100 ml) and reacted with Ra--N1 (1.5 g). Reduction under a pressure of 512 psi at 19.5° C. affords 5.9 g (60%) of 4-[-2-(-3,4-dibenzyloxyphenyl)ethyl]benzenamine, mp 97°-101° C.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04939133 |
| Source dataset | uspto-grants-1990_07 |
| ORD ID | ord-5b2c54497ecf4a9db3c418897e7f6826 |
| Source note | uspto-grants-1990_07 |