HuagongsheHuagongshe Chemistry Print Report · For research reference only
Ethanol → HCID 54155343, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Ethanol | HCID 702 | — |
| Reactant | Formaldehyde | HCID 712 | — |
| Reactant | N-Methyl-N-naphthylmethylamine | HCID 84474 | — |
| Solvent | Dichloromethane | HCID 6344 | — |
| Product | HCID 54155343 | HCID 54155343 | — |
Reaction Steps
21 g of N-methyl-1-naphthylmethylamine and 9 g of abs. ethanol are treated under ice-cooling in portions with 3.6 g of paraformaldehyde and the mixture stirred for 1 hour at room temperature. The reaction mixture is treated with dichloromethane, filtered and concentrated. The pure product is obtained as a pale yellow oil following vacuum distillation (1.3 mbar/135°-138°).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04939148 |
| Source dataset | uspto-grants-1990_07 |
| ORD ID | ord-aad9693db08d4404b0c9af732d5a26d5 |
| Source note | uspto-grants-1990_07 |