Tetrabutylammonium Fluoride → HCID 88522873, compound

Participants

Reaction Steps

In a manner similar to scheme V, 42 (0.13 gm) was treated with tetrabutylammonium fluoride and the product was purified by SiO2 with 1.5:1 EtOAc:hexanes as the eluent. Concentration in vacuo of the product rich fractions provided 0.51 gm of the product. mp 71°-77° C. Anal. C26H30FNO5 500 0.25 H2 0: Theory C: 67.89; H: 6.68; N: 3.04. Found C: 67.83; H: 6.95; N: 2.90.

Provenance & Evidence