HuagongsheHuagongshe Chemistry Print Report · For research reference only
Triethylamine → HCID 23043803, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Triethylamine | HCID 8471 | — |
| Reactant | Methanesulfonyl chloride | HCID 31297 | — |
| Reactant | HCID 23043978 | HCID 23043978 | — |
| Solvent | Dimethylformamide | HCID 6228 | — |
| Product | HCID 23043803 | HCID 23043803 | — |
Reaction Steps
Methanesulphonylchloride (0.41 ml) was added to a stirred solution of the Intermediate (a) (2.74 g) and triethylamine (0.74 ml) in dry dimethylformamide. The solution was stirred at room temperature for 10 hours.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04939147 |
| Source dataset | uspto-grants-1990_07 |
| ORD ID | ord-b0e0595fc8154689879a93c08068d3db |
| Source note | uspto-grants-1990_07 |