HuagongsheHuagongshe Chemistry Print Report · For research reference only
3-Chloro-1-propanol → 3-Hydroxypropyl Dimethyl Octadecyl Ammonium Chloride
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 3-Chloro-1-propanol | HCID 12313 | — |
| Reactant | Dimethyloctadecylamine | HCID 15365 | — |
| Solvent | Acetonitrile | HCID 6342 | — |
| Product | 3-Hydroxypropyl Dimethyl Octadecyl Ammonium Chloride | HCID 86744093 | 77.7% |
Reaction Steps
Employing the procedure of EXAMPLE II, 31.3 g of N,N-dimethyloctadecylamine was reacted with 9.0 g of 3-chloropropanol in 100 ml of acetonitrile to provide a crude product which was recrystallized from acetone to give 29.0 g (70%) of white solids. Proton NMR confirmed the desired structure.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04939289 |
| Source dataset | uspto-grants-1990_07 |
| ORD ID | ord-473c271b8a9b4ae0a0e7cfc45ed56c9c |
| Source note | uspto-grants-1990_07 |