HuagongsheHuagongshe Chemistry Print Report · For research reference only
N-Phenyl-p-phenylenediamine → HCID 15065940, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | N-Phenyl-p-phenylenediamine | HCID 7564 | — |
| Reactant | Ethyl orthoformate | HCID 31214 | — |
| Solvent | Ethanol | HCID 702 | — |
| Product | HCID 15065940 | HCID 15065940 | 83% |
Reaction Steps
The procedure of Example 1 is repeated using 10.0 g (0.054 mol) of N-phenyl-1,4-phenylenediamine and 3.3 g (0.22 mol) of triethyl orthoformate. The residue is slurried with ethanol to give 7.4 g (83%) of a brown solid, mp. 173°-175° C.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04939300 |
| Source dataset | uspto-grants-1990_07 |
| ORD ID | ord-2bffc21e40754691a7bbeb702e9ac2ac |
| Source note | uspto-grants-1990_07 |