HuagongsheHuagongshe Chemistry Print Report · For research reference only
HCID 54049138, compound → HCID 13316973, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | HCID 54049138 | HCID 54049138 | — |
| Catalyst | Platinum oxide (PtO) | HCID 82844 | — |
| Solvent | Ethanol | HCID 702 | — |
| Product | HCID 13316973 | HCID 13316973 | 98.3% |
Reaction Steps
A solution of 10.5 g of 4-(6-bromohex-3-enyl)benzonitrile in 200 ml of absolute ethanol was hydrogenated in the presence of 0.25 g of platinum oxide catalyst. Isolation of the product afforded 10.4 g of 4(6-bromohexyl)benzonitrile as a yellow oil which was distilled at 168°-170° C.(0.01 mm) to produce the compound as a colorless oil which solidified upon cooling.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04939267 |
| Source dataset | uspto-grants-1990_07 |
| ORD ID | ord-9f69ed0f573d4e0ca2c64afe2fc42d9e |
| Source note | uspto-grants-1990_07 |