HuagongsheHuagongshe Chemistry Print Report · For research reference only
3-(5-Methyl-1,2-oxazol-3-yl)propan-1-ol → 3-(5-Hydroxypentyl)-5-methylisoxazole
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 3-(5-Methyl-1,2-oxazol-3-yl)propan-1-ol | HCID 13316974 | — |
| Reactant | 3-(4-Carboxybutyl)-3-methylisoxazole | HCID 20064107 | — |
| Reactant | Aluminium lithium hydride | HCID 21226445 | — |
| Product | 3-(5-Hydroxypentyl)-5-methylisoxazole | HCID 13316977 | 84% |
Reaction Steps
3-(5-Hydroxypentyl)-5-methylisoxazole was prepared by reduction of 3-(4-carboxybutyl)-3-methylisoxazole with lithium aluminum hydride according to the procedure of part (e) above, and was obtained in 84% yield as an oil, b.p. 115°-125° C.(0.1 mm).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04939267 |
| Source dataset | uspto-grants-1990_07 |
| ORD ID | ord-45d3197fca5f4f9f86baf0378ad17182 |
| Source note | uspto-grants-1990_07 |