Ethyl 2-oxocyclohexylacetate → HCID 23043061, compound
Reaction equation
Cl.[CH3:2][O:3][C:4]1[CH:19]=[CH:18][C:7]([CH2:8][N:9]([C:11]2[CH:16]=[CH:15][C:14]([F:17])=[CH:13][CH:12]=2)N)=[CH:6][CH:5]=1.[CH3:20][CH2:21][O:22][C:23]([CH2:25][CH:26]1[C:31](=O)[CH2:30][CH2:29][CH2:28][CH2:27]1)=[O:24]>>[CH3:2][O:3][C:4]1[CH:19]=[CH:18][C:7]([CH2:8][N:9]2[C:27]3[CH:26]([CH2:25][C:23]([O:22][CH2:21][CH3:20])=[O:24])[CH2:31][CH2:30][CH2:29][C:28]=3[C:16]3[C:11]2=[CH:12][CH:13]=[C:14]([F:17])[CH:15]=3)=[CH:6][CH:5]=1Participants
3
Procedure
Following the procedure of Example 1, but using 1-(4-methoxybenzyl)-1-(4-fluorophenyl)hydrazine hydrochloride and ethyl 2-cyclohexanone acetate as starting materials, the title compound was prepared.
Sources & evidence
- ORD record
- ord-3f338dc3a6ed46ba8740c261606adc76
- Source dataset
- uspto-grants-1990_07
- Patent number
- US04940719
Reaction notes
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